I found this and found a really helpful thread on here regarding setting permissions from the command line.
Here is the thread-
viewtopic.php?f=160&t=25015And here is the relevant bit that helped me-
Personally - I haven't stuck to the web interface because it is fairly cumbersome and so have used SSH to access the DiskStation as root.
When you are this user you are all powerful and you can issue the following commands to restrict access to folders:
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chown -R user.group /volume1/homes/user-folder
where user, group and user-folder obviously need to be amended to what you want.
Then you can issue a:
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chmod -R 700 /volume1/homes/user-folder
restricting the access to the folder to just the user specified above.
Hope this helps!