Just in case others find this useful. I didnt trust using the usual method in updating ext3 to ext4 using tune2fs.
I bought a ds210j with 2 hard drives (WD Caviar Greens which is another story). I installed DSM 2.3 and formatted the drives as per instructions. Played around with it and then a found DSM 3 would be released soon so didnt copy much over until that was available.
After installing DSM 3 and backing up my data to a USB device (which worked fine for my purposes) I tried to delete the volume in the GUI but it would not do anything - it would just refresh the page and nothing would change. I then tried resetting DSM to its defaults (including format) but still didnt do anything. In the end I logged into the ds210j and ran:
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umount /volume1
cat /proc/mdstat
mdadm --misc --zero-superblock /dev/xxx
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/dev/xxx
will be the partitions being used for the raid device for /volume1 listed in
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/proc/mdstat
After a reboot the GUI didnt list my volume anymore and I could create a new volume. Looking at the volume after creation it is a LVM device and formatted with ext4. Not sure whether I need to add noatime to the mount options but will leave it for now.
This may help a few others - not sure whether the other raid partitions (/dev/md0 and /dev/md1) need updating (used for system purposes) but it all seems to work now.
Tom